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1 article(s) from Samsodien, Halima

Inclusion complexes of 2-methoxyestradiol with dimethylated and permethylated β-cyclodextrins: models for cyclodextrin–steroid interaction

Mino R. Caira,
Susan A. Bourne,
Halima Samsodien and
Vincent J. Smith

Beilstein J. Org. Chem. 2015, 11, 2616–2630, doi:10.3762/bjoc.11.281

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Graphical Abstract

Figure 1: Chemical structures of 2-methoxyestradiol (top) and the derivatised CDs DIMEB and TRIMEB (bottom).

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Figure 2: The mode of inclusion of 2ME in the DIMEB cavity (a), space-filling side view of the complex with t...

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Figure 3: Stereoview of the asymmetric unit in the crystal of the inclusion complex TRIMEB•2ME, with the host...

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Figure 4: Space-filling images of complex unit A (as representative of units A and B) (a) and complex unit C ...

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Figure 5: Inclination of the mean plane of the included 2ME molecule relative to the O4-heptagon of the host ...

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Figure 6: Overlay of the steroid nucleus of 2ME (blue) in its own crystal with the refined models (grey) of t...

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Figure 7: The TRIMEB·2ME complex unit D with two distinct (guest)O19-H···O(host) hydrogen bonds highlighted. ...

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Figure 8: Dissolution profiles in water at 37 °C for untreated 2ME and various β-CD-containing preparations o...

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Published 16 Dec 2015

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